ASTM a Test, Intergranular Corrosion, IGC, ASTM A Practice, Testing, India Ferric Sulfate – Sulfuric Acid, ASTM A – Practice B (Streicher Test). ASTM A practice – Free download as Excel Spreadsheet .xls /.xlsx), PDF File .pdf), Text File .txt) or read online for free. ASTM A Practice B test. In this test a sample of surface area cm. 2 is exposed for a period of hours to boiling solution of 50% H2SO4 + %.
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Methods for preparing the test a2662, rapid screening tests, apparatus setup and testing procedures, and calculations and report contents are described for each testing practice.
The test is generally performed for acceptance of materials, but not sufficient for rejection of materials. Intergranular corrosion is the proper use, though the specification calls it attack, corrosion is what is taking place.
ASTM A Testing: An Overview of Intergranular Corrosion | Element
From macroscopic imaging to Scanning Electron Microscopy, Element provides turnkey metallographic services using state-of-the-art equipment. Discover perspectives, resources, and advice from our world-leading Engaged Experts. This test is used exclusively to determine corrosion in areas high practic chromium carbide formations, and is not as effective for intergranular attack caused by other means.
Practice E, the Strauss test, is performed to assess attack associated with chromium-rich carbide formation; it does not detect susceptibility to sigma phase formation.
In everyday applications, corrosion varies by materials and solutions. The bent samples are examined at low magnification, where the appearance of cracks or fissures indicate intergranular attack. In many cases we can reduce that to as little as 24 hours more than the required testing time if you need fast results.
The Oxalic Acid test is only used to ensure that no corrosion exists; samples are labeled either “Acceptable” or “Suspect”. Historical Version s – view previous versions of standard Aztm Item s – proposed revisions of this standard Translated Version s: Sensitization causes the grain boundaries of a material to precipitate, creating carbide deposits and causing the material to be susceptible to intergranular attack.
Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard. Link to Active This link will always route to the current Active version of the standard.
A different ASTM A test method must be used to quantify the level of corrosion or to disqualify a material for use. Rockwell or Superficial Hardness. Due to the variance of attack in different materials, numerous methods Practices B-F are used to assess intergranular corrosion. Astmm to the Streicher test, the Huey test method uses a nitric acid solution and subjects the specimen to five hour boiling intervals.
The etch structure types used to classify the specimens are: In SEM analysis, intergranular corrosion is clear by the dark lines where the grain boundaries are eaten away. The Strauss test is commonly used to evaluate the heat-treatment of as-received material, the effectiveness of alloying additions of elements such as Nb and Ti, or the effectiveness of reducing carbon content to resist intergranular attack.
Intergranular simply means that the corrosion is taking place between the grains or crystals, which is where sigma phase or chromium carbides are going to form which makes the material susceptible to IGA. It is informational only and not an official part of the standard; the full text of the standard itself must be referred to for its use and application.
Carbon and Sulfur Analysis. This specification is for detecting susceptibility to intergranular attack IGA. ASTM does not give any warranty express or implied or make any representation that the contents of this abstract are accurate, complete or up to date. To understand intergranular corrosion testing or intergranular attack commonly abbreviated as IGC or IGAit is important to understand what causes the process to occur.
Intergranular corrosion occurs as a result of precipitation of nitridescarbidesand other intermetallic phasessuch as sigma phase, that occurs along the grain boundaries. Learn more about our laboratories – where they are located; the unique capabilities they have and how they can help you solve your technical and commercial challenges. Duplicate samples practic both sides of a sheet sample are evaluated to determine if carburization results in intergranular attack.
Strauss test specimens are boiled in a Copper Sulfate – Sulfuric Acid mixture for 15 hours.
Because it can be run quickly for screening, we often run this test first. Please specify the maximum allowable corrosion rate and any available data on the sensitizing heat treatment performed. Praactice practices include five intergranular corrosion tests, namely: If materials with incorrect heat treatment enter service, they are liable to crack or fail by intergranular corrosion IGC much more rapidly than properly treated materials; ASTM A is a screening test to help find batches that are incorrectly processed.
Practice F, is a hour weight-loss based analysis that provides a quantitative measure of the materials performance, and is commonly used ast analyze as-received stainless steels. The test evaluates the resistance of extra-low-carbon steels to sensitization and intergranular attack from welding or heat treatment processes.
Contact us now for pricing or a quote! The oxalic acid test is commonly used before the Strauss test to determine pracyice a sample is susceptible; samples that pass method A will generally show low corrosion rates in the Strauss test.