Add Attachments to Content Item ‘ASTM D Glass Transition Temperature ( DMA Tg) of Polymer Matrix Composites by Dynamic Mechanical Analysis (DMA) . ASTM D Glass Transition Temperature (DMA Tg) of Polymer ASTM D has become a widely used test standard in many companies due to. ASTM D用DMA测试Tg_能源/化工_工程科技_专业资料。Designation: D – 07?1 Standard Test Method for Glass Transition.
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The span-to-depth ratio, ply orientation, and ply stacking sequence of a specimen with respect to the testing? The two tangent lines are intersected, and temperature corresponding to this intersection point is recorded as the DMA Tg. D — 07? See Appendix X1 for additional guidelines to draw tangent lines. Current edition approved Dec. Determination and Report of Procedures. On the other hand, if the two tangent lines are constructed at temperatures too far away from the transition, the intersection is depicted in Fig.
Any deviations from this heating rate shall be noted in the report atsm the result shall be reported as non-standard.
A number in parentheses indicates the year of last reapproval. D Terminology for Plastics: Therefore, it is recommended that the test specimens should be weighed before and after DMA Tg testing to quantify the moisture change in the specimen resulting axtm the DMA Tg test. The materials listed in Table 1 are de? A non-standard specimen con?
If d0728 different heating rate is used it shall be described in the report and the result recorded as nonstandard. In general, for a given material, a higher testing frequency produces a higher DMA Tg value than this standard, while use of the resonance mode will yield a different DMA Tg that may be either higher or lower than the standard.
Before the transition the storage modulus is relatively constant, the sigmoidal change during transition is clear, and after the transition the storage modulus is relatively constant.
It is possible that more than one transition exists, but this should be con? ASTM E The temperature calibration points astmm span the DMA Tg result. A change in heating rate will affect the glass transition temperature result; the standard heating rate is the best available compromise for comparing DMA Tg results of dry and wet laminates. This temperature is designated as TB.
These averages allow a relative comparison of the repeatability within laboratory precision and reproducibility between laboratory precision of the DMA Tg test parameters. Work Item s – proposed revisions of this standard. A meaningful comparison of data requires that the specimen con? Interpretation of Results Using this approach the intersection point is drawn as shown in Fig. Your comments are invited either for revision of this standard or for additional standards and should be addressed to ASTM International Qstm.
Strains of less than 0. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Precision and Bias 4 Examples are shown in this appendix to provide graphical illustrations of how to select the two tangent lines. Individual reprints single or multiple copies of this standard may be obtained by contacting ASTM at the above address or at phonefaxor service astm.
The temperature at which a signi? Generally, the specimen should be centered between the clamp faces and be parallel to the base of the instrument. Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard.
ASTM D7028 – 07(2015)
Weigh the specimen to the nearest milligram 0. Record any visual anomalies observed. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the risk of infringement of such rights, are entirely their own responsibility.
Depending on the analyzer, typical specimen size can range from 56 6 4 3 12 6 1 3 2. If the testing is part of a designed experiment, other sampling techniques may be used if described in the test plan.
The conditioned specimens shall be tested within 30 minutes after removal from the conditioning chamber, or stored in sealed MIL-PRF or equivalent aluminized bag until test. A non-standard DMA Tg de? Table 1 presents the precision statistics generated from this study as de?